HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → HCID 4778525, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 178465579 | HCID 178465579 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 4778525 | HCID 4778525 | — |
Reaction Steps
The intermediate 7 was prepared by the same procedure for the intermediate 6, using a intermediate 5 (2.7 g, 14.6 mmol), chloroacetyl chloride (2.37 mL, 30.0 mmol) and triethylamine. After normal workup, the pure title compound was obtained by recrystallization from MeOH as a white solid (3.44 g, 90%):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05990126 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-6fb9d4a073be406da905d879f9d51de7 |
| Source note | uspto-grants-1999_11 |