Triethylamine → HCID 18005169, compound

HRID 1603764Notes

Reaction equation

HRID 1603764 reaction equation
[CH2:1]([C:3]1[CH:4]=[C:5]([CH:7]=[C:8]([C:10]2[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=2)[CH:9]=1)[NH2:6])[CH3:2].Cl[C:17]([O:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)=[O:18].C(N(CC)CC)C>ClCCl>[CH2:1]([C:3]1[CH:4]=[C:5]([NH:6][C:17](=[O:18])[O:19][C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:7]=[C:8]([C:10]2[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=2)[CH:9]=1)[CH3:2]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 15891Phenyl chloroformateHCID 18005134HCID 18005134, compound

Product 1

HCID 18005169HCID 18005169, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

The title compound (0.276 g, 0.87 mmol) was prepared by the methodology of description 67, using 3-ethyl-5-(pyrid-3-yl)aniline, phenyl chloroformate (0.13 ml, 0.96 mmol) and triethylamine (0.13 ml, 0.96 mmol) in dichloromethane (10 ml)

Sources & evidence

ORD record
ord-d57aac9cbc7846aba750329004f87c65
Source dataset
uspto-grants-1999_11
Patent number
US05990133

Reaction notes

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