HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 22004117, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 70247570 | HCID 70247570 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 22004117 | HCID 22004117 | 77% |
Reaction Steps
Demethylation of 4-methoxy-1-phenylbenzimidazole hydrochloride with HBr in glacial acetic acid as described for synthesis of Example 2 gave Example 11 as the HCl salt, (77%): mp (MeOH/Et2O) 238-240° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05990146 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-db31e96638a44264a84d9ff9b645a95e |
| Source note | uspto-grants-1999_11 |