HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Benzyloxymethyl)-6-chromanecarboxylic acid → Methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Benzyloxymethyl)-6-chromanecarboxylic acid | HCID 19606251 | — |
| Reactant | HCID 178507421 | HCID 178507421 | — |
| Product | Methanol | HCID 887 | 57% |
| Product | HCID 178521894 | HCID 178521894 | — |
Reaction Steps
Following the process described in example 1 (point K), starting from 2-(benzyloxymethyl)-6-chromanecarboxylic acid and 8-amino-4-oxo-2-(5-1H-tetrazolyl)-4H-1-benzopyran, the title compound was prepared as a white solid with melting point 214-216° C., which was purified by crystallization in methanol (57% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05990142 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-f6e22a73f39341e7a2428afa46aa3f31 |
| Source note | uspto-grants-1999_11 |