HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19606307, compound → Methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19606307 | HCID 19606307 | — |
| Reactant | HCID 178507421 | HCID 178507421 | — |
| Product | Methanol | HCID 887 | 65% |
| Product | HCID 178521893 | HCID 178521893 | — |
Reaction Steps
Following the process described in example 2 (point K), starting from 2-(3-phenylpropyl)-6-chromanecarboxylic acid and 8-amino-4-oxo-2-(5-1H-tetrazolyl)-4H-1-benzopyran, the title compound was prepared as a white solid which decomposes at temperatures higher than 370° C. and which was purified by crystallization in methanol (65% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05990142 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-0f1eddfa76b8474fa2ce1eb7e4d1f5ce |
| Source note | uspto-grants-1999_11 |