HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethyl bromide → HCID 19606320, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethyl bromide | HCID 7666 | — |
| Reactant | HCID 19606269 | HCID 19606269 | — |
| Product | HCID 19606320 | HCID 19606320 | 58% |
Reaction Steps
Following the process described in example 3 (point B), starting from ethyl 7-chloro-2-trifluoromethanesulfonyloxymethyl-2,3-dihydrobenzofuran-5-carboxylate and 2-bromoethylbenzene, the title compound was prepared, which was purified by chromatography through a silica gel column, eluting with petroleum ether:ethyl acetate, 95:5 (58% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05990142 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-4d3b7e67f8e343268f04d0584a4771d5 |
| Source note | uspto-grants-1999_11 |