HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Oxalate → Ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Oxalate | HCID 7268 | — |
| Reactant | HCID 19606348 | HCID 19606348 | — |
| Product | Ethanol | HCID 702 | 55% |
| Product | HCID 19606340 | HCID 19606340 | — |
Reaction Steps
Following the process described in example 1 (point A), starting from N-(3-acetyl-5-fluoro-2-hydroxyphenyl)-2-(3-phenylpropyl)-2,3-dihydrobenzofuran-5-carboxamide and diethyl oxalate, the title compound was prepared, which was purified by crystallization in ethanol (55% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05990142 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-bd9c194321024850889bdedc284aaa01 |
| Source note | uspto-grants-1999_11 |