HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-2-hydroxyacetophenone → HCID 19606273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-2-hydroxyacetophenone | HCID 459294 | — |
| Reactant | HCID 19606252 | HCID 19606252 | — |
| Product | HCID 19606273 | HCID 19606273 | 42% |
Reaction Steps
Following the process described in example 1 (point K), starting from 6-chloro-2-(3-phenylpropyl)-2,3-dihydrobenzofuran-5-carboxylic acid and 3-amino-2-hydroxyacetophenone, the title compound was prepared, which was purified by chromatography through a silica gel column, eluting with hexane:ethyl acetate, 1:1 (42% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05990142 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-0cda1be28ce74763ad8a1be4ededc2ae |
| Source note | uspto-grants-1999_11 |