HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenebutanol → HCID 19606259, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenebutanol | HCID 76889 | — |
| Reactant | Methyl 2-fluoro-4-hydroxybenzoate | HCID 22463192 | — |
| Product | HCID 19606259 | HCID 19606259 | 97% |
Reaction Steps
Following the process described in example 18 (point A), starting from methyl 2-fluoro-4-hydroxybenzoate and 4-phenyl-1-butanol, the title compound was prepared, which was purified by chromatography through a silica gel column, eluting with hexane:ethyl acetate, 95:5 (97% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05990142 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-62a8419acf474dba82c5a170cf42a853 |
| Source note | uspto-grants-1999_11 |