HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 19606247, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 70149208 | HCID 70149208 | — |
| Product | HCID 19606247 | HCID 19606247 | 83% |
Reaction Steps
Following the process described in example 18 (point C), starting from ethyl 2-(4'-fluorobenzyloxymethyl)-2,3-dihydrobenzofuran-2-carboxylate (7.00 g, 23.2 mmol), LiAlH4 (3.51 g, 92.6 mmol) and dry ethyl ether (300 ml), the title compound was prepared (83% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05990142 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-8d2c533ae4ee40c7ae9325c07e0f43e6 |
| Source note | uspto-grants-1999_11 |