Indene → HCID 178506815, compound

HRID 1603970Notes

Reaction equation

[CH2:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1.[Li:10]CCCC>>[CH:1]1([Li:10])[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1

Participants

Reactant 2

HCID 7219Indene

HCID 178418339Butyllithium

Product 1

HCID 178506815HCID 178506815, compound

Procedure

Indene was reacted with BuLi to form indenyl lithium, which compound was reacted with methyl iodide to form 1-methylindene. Use was made of: 18.2 grams of indene, 100 ml of n-BuLi solution, 22.0 grams of methyl iodide.

Sources & evidence

ORD record: ord-3e46c9ba538d4e60a17b3ed2f6b621b9
Source dataset: uspto-grants-1999_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05990253

Reaction notes

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