Dichloromethane → HCID 15434936, compound

Participants

Reaction Steps

In 30 ml of dichloromethane suspended with 1.00 g of 2-(3,5-dichlorophenyl)-2,3,4,5-tetrahydro-1,2,4-triazine-3,5-dione followed by addition of 2-fold morlar each of carbone tetrachloride and triphenylphosphine and refluxed for 12 hours. After the completion of the reaction, the resulted solution were purified by column chromatography (Merck Silica Gel 60 dichloromethane-carbontetrachloride=2:1). m.p. 148-149° C.

Provenance & Evidence