Butyl iodide → Butyl 6-[N-(5-bromo-2-butoxybenzyl)-N-ethylamino]pyridazine-3-carboxylate

HRID 1604377Notes

Reaction equation

I[CH2:2][CH2:3][CH2:4][CH3:5].[Br:6][C:7]1[CH:8]=[CH:9][C:10]([OH:30])=[C:11]([CH:29]=1)[CH2:12][N:13]([C:16]1[N:21]=[N:20][C:19]([C:22]([O:24][CH2:25][CH2:26][CH2:27][CH3:28])=[O:23])=[CH:18][CH:17]=1)[CH2:14][CH3:15]>>[Br:6][C:7]1[CH:8]=[CH:9][C:10]([O:30][CH2:2][CH2:3][CH2:4][CH3:5])=[C:11]([CH:29]=1)[CH2:12][N:13]([C:16]1[N:21]=[N:20][C:19]([C:22]([O:24][CH2:25][CH2:26][CH2:27][CH3:28])=[O:23])=[CH:18][CH:17]=1)[CH2:14][CH3:15]

Participants

Reactant 2

HCID 10962Butyl iodide

HCID 22622486butyl 6-[N-(5-bromo-2-hydroxybenzyl)-N-ethylamino]pyridazine-3-carboxylate

Product 1

HCID 22622492Butyl 6-[N-(5-bromo-2-butoxybenzyl)-N-ethylamino]pyridazine-3-carboxylate

Procedure

The title compound was prepared by reacting 1-iodobutane and butyl 6-[N-(5-bromo-2-hydroxybenzyl)-N-ethylamino]pyridazine-3-carboxylate using a similar method to that of reference example 4.

Sources & evidence

ORD record: ord-52c52e485cf244c38e4b2678e0f5c762
Source dataset: uspto-grants-1999_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05994353

Reaction notes

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