HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15887567, compound → Ethyl 4-(2-hydroxyphenoxy)butanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15887567 | HCID 15887567 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 4-(2-hydroxyphenoxy)butanoate | HCID 15887568 | — |
Reaction Steps
A mixture of (3) (1.57 g, 5.0 mM), ethanol (50 mL), glacial acetic acid (7 drops) and 10% palladium on carbon (0.7 g) was reacted in a hydrogen atmosphere (40 p.s.i.) at room temperature until hydrogen uptake ceased. Concentration of the filtered mixture yielded the product (4) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05994362 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-b113687707d1434e8257e6643a54ff55 |
| Source note | uspto-grants-1999_11 |