Sodium Hydroxide → HCID 15434168, compound

Participants

Reaction Steps

To a solution of 14c (38 mg, 0.13 mmol) in methanol (3 mL) was added 2N NaOH (0.1 mL, 0.2 mmol). The light yellow solution was stirred overnight, then concentrated. The residue was partitioned between pH 7 phosphate buffer and EtOAc. The organic phase was washed with brine, dried over MgSO4 and evaporated to provide 31 mg of the title compound as an oil.

Provenance & Evidence