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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1604542Generated: November 1, 2026

HCID 19603423, compound → HCID 19603369, compound

https://huagongshe.com/reaction/1604542

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 19603423HCID 19603423—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
SolventWaterHCID 962—
ProductHCID 19603369HCID 19603369—

Reaction Steps

The residue including benzyl 2-(2-methyl-3-pyridyl)acetate obtained in Preparation 29-(2) was dissolved in methanol (5 ml), and 10% palladium on carbon was added thereto. The mixture was stirred under hydrogen atmosphere for 3 hours. The reaction mixture was diluted with water and washed with ethyl acetate. The solvent was removed in vacuo to give 2-(2-methyl-3-pyridyl)acetic acid (90 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05994368
Source datasetuspto-grants-1999_11
ORD IDord-935d536c34d74ca998dcede237776da7
Source noteuspto-grants-1999_11