HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 19603381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 19603263 | HCID 19603263 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19603381 | HCID 19603381 | 49.9% |
Reaction Steps
A mixture of 8-[3-[N-[2-(4-aminophenylthio)-acetylglycyl]-N-methylamino]-2,6-dichlorobenzyloxy]-2-methylquinoline (56 mg) triethylamine (15 mg), and acetic anhydride (15 mg) in dichloromethane (2 ml) was stirred for 4 hours at ambient temperature. The resulting precipitates were collected by filtration to give 8-[3-[N-[2-(4-acetamidophenylthio)acetylglycyl]-N-methylamino)-2,6-dichlorobenzyloxy]-2-methylquinoline (30 mg) as a colorless crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05994368 |
| Source dataset | uspto-grants-1999_11 |
| ORD ID | ord-7fee253bbe33403c80874a20424da59e |
| Source note | uspto-grants-1999_11 |