反应详情

温度

100 °C

Dry 1-methylimidazole (9.03 g, 0.11 mol) was mixed with 1-chlorohexane (12.06 g, 0.1 mol) and placed in a Corius tube inside a dry box. The Corius tube was then closed using a super seal in the dry box and sealed under vacuum. The two components formed two layers, inside the Corius tube, and this mixture was heated at 100° C. for a week. The resulting product was allowed to cool to room temperature when it formed a viscous product. The viscous product was transferred from the dry box to a Schlenk round bottomed flask where it was left under vacuum for 4 hours to form a viscous liquid.

1. customplaced in a Corius tube inside a dry box
2. customThe Corius tube was then closed
3. customa super seal in the dry box
4. customsealed under vacuum
5. customThe two components formed two layers
6. temperatureto cool to room temperature when it
7. customformed a viscous product
8. customThe viscous product was transferred from the dry box to a Schlenk round bottomed flask
9. customto form a viscous liquid