1-Methylimidazole → HCID 178444699, compound

Participants

Reaction Conditions

Reaction Steps

Dry 1-methylimidazole (9.03 g, 0.11 mol) was mixed with 1-chlorohexane (12.06 g, 0.1 mol) and placed in a Corius tube inside a dry box. The Corius tube was then closed using a super seal in the dry box and sealed under vacuum. The two components formed two layers, inside the Corius tube, and this mixture was heated at 100° C. for a week. The resulting product was allowed to cool to room temperature when it formed a viscous product. The viscous product was transferred from the dry box to a Schlenk round bottomed flask where it was left under vacuum for 4 hours to form a viscous liquid.

Provenance & Evidence