HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 131710120, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | HCID 131710121 | HCID 131710121 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 131710120 | HCID 131710120 | — |
Reaction Steps
3-Chloro-5-[2-(dimethylamino)ethyl]-2-phenyl-1,5-benzothiazepin-4(5H)-one, hydrochloride (prepared as described in Example 1) is treated with one equivalent of hydrogen peroxide in dilute acetic acid, and allowed to stand for about 16 hours. Solvent removal yields the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03948889 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-3a6f266433fd471485ffa9c6df3da035 |
| Source note | uspto-grants-1976_04 |