HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → AGN-PC-0NICCC
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | HCID 12786149 | HCID 12786149 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | AGN-PC-0NICCC | HCID 12279087 | 93.7% |
Reaction Steps
In ethanol (10 ml) was dissolved ethyl 1,2-benzisoxazole-3-acetimidate hydrochloride (2.0 g) and thereto was added ethylenediamine (0.6 g) under ice-cooling and the mixture was allowed to stand at 5°C overnight. To the mixture was added ethanolic hydrochloric acid and the precipitated crystallines were separated by filtration and recrystallized from ethanol to give the desired compound (1.85 g). m.p. 223° to 228°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03948928 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-0481f6b948d249ea98299821104a247b |
| Source note | uspto-grants-1976_04 |