HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 21400841, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 178496910 | HCID 178496910 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21400841 | HCID 21400841 | — |
Reaction Steps
A mixture of 3.0 g 3-(2-carbomethoxy-1-cyclohexen-1-yl)-5-phenylpyrazole, 0.3 g of 50% sodium hydride-mineral oil slurry, and 1.0 g of methyl iodide in 50 ml of anhydrous tetrahydrofuran is stirred and refluxed overnite. The reaction mixture is filtered, and the solvent is evaporated from the filtrate to give 1-methyl-3-(2-carbomethoxy-1-cyclohexen-1-yl)-5-phenylpyrazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03948937 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-2edb842c44e94845bc27fbec4ad0e9a5 |
| Source note | uspto-grants-1976_04 |