HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 178484366, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | 1,1,3,3-Tetramethylguanidine | HCID 66460 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 178484366 | HCID 178484366 | — |
Reaction Steps
Tetramethylguanidine (22 g., 0.19 mole) was dissolved in anhydrous ether (100 ml.) and to this solution at 0° was added a solution of anhydrous formic acid (7.1 ml., 0.198 mole) in anhydrous ether (40 ml.). The resulting salt crystallized. It was collected, washed with ether, dried in high vacuum and recrystallized from chloroform-ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03948927 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-955a2edaee774b559658155b74868ef6 |
| Source note | uspto-grants-1976_04 |