Methane → HCID 21548856, compound

Participants

Reaction Conditions

Reaction Steps

A mixture consisting of 10 gm (0.056 mol) of N-benzoyl-glycine and 10.5 gm (0.056 mol) of n-dodecyl-amine was heated for 90 minutes at 160°C., while stirring. Thereafter, ethyl acetate and activated charcoal were added to the reaction mixture, and the mixture was vacuum-filtered while still hot. Upon cooling of the filtrate, a crystalline substance separated out which was collected and again recrystallized from ethyl acetate, yielding 11.9 gm (58% of theory) of the compound of the formula ##EQU4## having a melting point of 124°C.

Provenance & Evidence