1,2-Ethanedithiol → HCID 2799043, compound

HRID 1605037Notes

Reaction equation

HRID 1605037 reaction equation
[C:1]([C:5]1[CH:6]=[C:7]([CH:10]=[C:11]([C:14]([CH3:17])([CH3:16])[CH3:15])[C:12]=1[OH:13])[CH:8]=O)([CH3:4])([CH3:3])[CH3:2].[CH2:18]([SH:21])[CH2:19][SH:20]>>[OH:13][C:12]1[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])=[CH:6][C:7]([CH:8]2[S:21][CH2:18][CH2:19][S:20]2)=[CH:10][C:11]=1[C:14]([CH3:17])([CH3:16])[CH3:15]

Participants

3

Reactant 2

HCID 109021,2-EthanedithiolHCID 732193,5-Di-tert-butyl-4-hydroxybenzaldehyde

Product 1

HCID 2799043HCID 2799043, compound

Procedure

Molar amounts of 3,5-di-tert.butyl-4-hydroxy benzaldehyde and 1,2-ethane dithiol are condensed by the method described in Example 1 to yield the 2-(4'-hydroxy-3', 5'-di-tert.butyl phenyl)-1,3-dithiolane of formula VII, ##SPC6##

Workup

  1. customcondensed by the method

Sources & evidence

ORD record
ord-621c7785eba744f2b6e1fb200939b78b
Source dataset
uspto-grants-1976_04
Patent number
US03948946

Reaction notes

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