Hydrogen iodide → HCID 21548938, compound

HRID 1605059Notes

Reaction equation

HRID 1605059 reaction equation
O[CH:2]1[C:15]2[CH:14]=[C:13]([CH:16]([CH3:19])[CH2:17][OH:18])[CH:12]=[CH:11][C:10]=2[O:9][C:8]2[C:3]1=[CH:4][CH:5]=[CH:6][CH:7]=2.I>C(O)(=O)C>[CH:14]1[C:15]2[CH2:2][C:3]3[C:8](=[CH:7][CH:6]=[CH:5][CH:4]=3)[O:9][C:10]=2[CH:11]=[CH:12][C:13]=1[CH:16]([CH3:19])[CH2:17][OH:18]

Participants

4

Reactant 2

HCID 24841Hydrogen iodideHCID 21548907HCID 21548907, compound

Product 1

HCID 21548938HCID 21548938, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

A mixture of 10 g. of 2-(9-hydroxy-2-xanthenyl)-propanol, 45 ml. of acetic acid, and 20 g. of concentrated hydriodic acid is refluxed for 3 minutes. After removal of the solvent by evaporation, 2-(2-xanthenyl)-propanol is obtained, m.p. 86°-89°.

Workup

  1. additionA mixture of 10 g
  2. customAfter removal of the solvent
  3. customby evaporation

Sources & evidence

ORD record
ord-c05e13458e3f4d7fbe70e9751572efad
Source dataset
uspto-grants-1976_04
Patent number
US03948949

Reaction notes

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