Benzaldehyde → HCID 474291, compound

HRID 1605063Notes

Reaction equation

HRID 1605063 reaction equation
[CH:1](=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[SH:9][CH:10]([CH2:13][SH:14])[CH2:11][OH:12]>>[OH:12][CH2:11][CH:10]1[CH2:13][S:14][CH:1]([C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[S:9]1

Participants

3

Reactant 2

HCID 240BenzaldehydeHCID 3080Dimercaprol

Product 1

HCID 474291HCID 474291, compound

Procedure

According to the procedure of Example 1, 35 g. (0.33 mole) of benzaldehyde and 40 g. (0.33 mole) of 2,3-dimercaptopropanol were reacted to yield 63.6 g. of crude product. After recrystallization 42.4 (56%) of the desired product were obtained as shown by nmr spectroscopy.

Workup

  1. customto yield 63.6 g
  2. customAfter recrystallization 42.4 (56%) of the desired product
  3. customwere obtained

Sources & evidence

ORD record
ord-06d67170767d42f799eb27100edd6b5c
Source dataset
uspto-grants-1976_04
Patent number
US03948944

Reaction notes

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