HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 21549153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 21549164 | HCID 21549164 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 21549153 | HCID 21549153 | — |
Reaction Steps
p-(2,2-Difluoro-1-methylcyclopropyl)phenol was prepared from 9.9 g. of p-(2,2-difluoro-1-methylcyclopropyl)anisole and 20 g. of boron tribromide in 200 ml. of ethylene dichloride according to the procedure described above in Example 1, part (c), affording 9 g. of pinkish oil which solidified upon standing.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03948973 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-55347b7689fd492fbc5294e734c9edf0 |
| Source note | uspto-grants-1976_04 |