HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 21549140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Benzene, 1-methoxy-4-(2-methyl-1-propenyl)- | HCID 11321128 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Pentane | HCID 8003 | — |
| Product | HCID 21549140 | HCID 21549140 | — |
Reaction Steps
p-(2,2-Dichloro-3,3-dimethylcyclopropyl)anisole was prepared from 58.3 g. of p-(2,2-dimethylvinyl)anisole, 102 g. of potassium t-butoxide, 180 ml. of chloroform and 1800 ml. of pentane according to the procedure described above in Example 1, part (b). The product was recrystallized from hexane to produce p-(2,2-dichloro-3,3-dimethylcyclopropyl)anisole in the form of colorless needles, m.p. 54.5°-57°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03948973 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-d34481a1029547a791d15722cd32c746 |
| Source note | uspto-grants-1976_04 |