HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 21549171, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 21549140 | HCID 21549140 | — |
| Product | HCID 21549171 | HCID 21549171 | — |
Reaction Steps
p-(2,2-Dichloro-3,3-dimethylcyclopropyl)phenol was prepared from 65.8 g. of p-(2,2-dichloro-3,3-dimethylcyclopropyl)anisole and 37.5 g. of boron tribromide according to the procedure described above in Example 1, part (c). There was thus obtained 23.5 g. of p-(2,2-dichloro-3,3-dimethylcyclopropyl)phenol, m.p. 111°-111.5°C. when recrystallized from a benzene-hexane mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03948973 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-8216fbd384a14f02bf66430727b93b9c |
| Source note | uspto-grants-1976_04 |