Sodium Hydroxide → HCID 21546685, compound

Participants

Reaction Steps

To 4.1 g of 3-morpholino-sydnonimine hydrochloride dissolved in 10 ml of water is added with stirring 1.440 g of 40% aqueous sodium hydroxide. The reaction mixture is stirred for 1 hour. The aqueous solution is concentrated and cooled. Two crops of crystals are collected, combined and recrystallized from a 2 to 1 solution of chloroform and methanol. Two crops of the purified product, α-(N-morpholino-N-nitrosoamino)acetamide, m.p. 134° - 136° C., are collected.

Provenance & Evidence