HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → Dipropyl peroxydicarbonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Sodium Chloride | HCID 5234 | — |
| Reactant | Propyl chloroformate | HCID 7998 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Product | Dipropyl peroxydicarbonate | HCID 85264 | — |
Reaction Steps
Using the apparatus (i.e., both centrifuges 18 and 30) and procedure of Example I (except that the temperature of reactor 14 is 25 ± 1° C.), NPP is prepared at the rate of 50 pph in an average assay of greater than 98% from 85 pph of n-propyl chloroformate, 31 pph of 50% aqueous H2O2, 169 pph of 20% NaOH and 50 pph of saturated NaCl solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03950375 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-195b029a725b461bac802e58a9d720c1 |
| Source note | uspto-grants-1976_04 |