HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → HCID 21520083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Sodium benzenethiolate | HCID 4110039 | — |
| Reactant | HCID 21520055 | HCID 21520055 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21520083 | HCID 21520083 | — |
Reaction Steps
A mixture of ethyl 3-benzylthio-4-chloro-5-sulfamylbenzoate (0.77 g), thiophenol (0.36 ml), and dry ethanol (15 ml) containing 3 millimoles of sodium thiophenolate is refluxed for 20 hours. After cooling the precipitate is collected by filtration to yield ethyl 3-benzylthio-4-phenylthio-5-sulfamylbenzoate with a melting point of 151°- 152° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03950376 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-fd64652a6e134f27affb7e6007f9ff31 |
| Source note | uspto-grants-1976_04 |