HCID 178418361, compound → HCID 178511262, compound

Participants

Reaction Steps

5 g. of trans-4-cyanocyclohexane-1-carboxylic acid was dissolved in 130 ml of methanol. To this solution, 5 g. of 10 % Pd-charcoal was added and the mixture was shaken in an atmosphere of hydrogen under a normal pressure for about 8 hours until 0.066 mole of hydrogen was absorbed. The reaction product was treated as described in Example 1, and 3.5 g. of trans-4-aminomethylcyclohexane-1-carboxylic acid was obtained.

Provenance & Evidence