HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Benzyloxy-5-nitro-4-phenylbenzoic acid → 5-Amino-3-isopentylthio-4-phenylbenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Benzyloxy-5-nitro-4-phenylbenzoic acid | HCID 21546844 | — |
| Reactant | 3-Isopentylthio-5-nitro-4-phenylbenzoic acid | HCID 21546849 | — |
| Product | 5-Amino-3-isopentylthio-4-phenylbenzoic acid | HCID 21546886 | — |
Reaction Steps
By replacing in Example 2, step D, 3-benzyloxy-5-nitro-4-phenylbenzoic acid with 3-isopentylthio-5-nitro-4-phenylbenzoic acid, and following the procedure described, 5-amino-3-isopentylthio-4-phenylbenzoic acid is obtained crystallizing with 0.25 mole of water with a melting point of 124.5°-125.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03950380 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-54b8142f2a1b4d4aa86c3dbeb1b51fef |
| Source note | uspto-grants-1976_04 |