Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 53728375 | HCID 53728375 | — |
| Product | HCID 20319037 | HCID 20319037 | — |
Reaction Steps
2.7 gm of 2-amino-3-bromo-5-carbomethoxy-N-ethyl-benzylamine were boiled for 35 minutes with 65 ml of 6 N hydrochloric acid. Thereafter, upon cooling the reaction solution to -15°C, N-ethyl-2-amino-3-bromo-5-carboxy-benzylamine hydrochloride crystallized out and was recrystallized from ethanol/ether, whereupon it had a melting point of 261°C (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US03950393 |
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| Source dataset | uspto-grants-1976_04 |
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| ORD ID | ord-454c258012f048a4a714c14a1f5daad4 |
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| Source note | uspto-grants-1976_04 |
|---|
