HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 22760978, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 22760937 | HCID 22760937 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 22760978 | HCID 22760978 | — |
Reaction Steps
6.2 g of 2-keto-1,2,3,4-tetrahydro-tribenzo(b,d,f)-oxepine are added to a suspension of 3.7 g of lithiumaluminiumhydride in 300 ml of dry ether. After refluxing for 2 hours 14.8 ml of water are added carefully. The suspension obtained is filtered off and after that the filtrate is dried and evaporated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03950425 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-40a252d0c60f46e7984a0e90e2e9ff6d |
| Source note | uspto-grants-1976_04 |