HRID1605667

反应详情

EQUATION

反应方程式

REACTANTS

反应物

$结构：CCOC(=O)/C=C(\C)OCC$

HCID5354173

Ethyl (2E)-3-ethoxy-2-butenoate

C8H14O3

HCID21484428

未命名化合物

PRODUCTS

生成物

$结构：CC(=O)/C=C(\C)c1ccc(C2CCCCCC2)c(Cl)c1$

HCID68135195

未命名化合物

收率 51%

PROCEDURE

实验过程

(E)-4-(3-chloro-4-cycloheptyl-phenyl)-3-pentene-2-one was prepared analogous to Example 52 from 3'-chloro-4'-cycloheptyl-acetophenone (b.p. 136°-139°C at 0.1 mm Hg; nD23 = 1.5572) and ethyl (E)-3-ethoxy-crotonate with a yield of 51% of theory. B.p. 160°-165°C at 0.1 mm Hg.