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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1605826Generated: November 3, 2026

Triethylamine → HCID 22789093, compound

https://huagongshe.com/reaction/1605826

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantChloroiodomethaneHCID 11644—
ReactantN-tert-Butoxycarbonyl-L-tryptophanHCID 83169—
SolventDimethylformamideHCID 6228—
ProductHCID 22789093HCID 22789093—

Reaction Steps

The compound was prepared by the method of Example 7A from N-tert.butoxycarbonyl-tryptophan, triethylamine, and chloroiodomethane in dimethylformamide; reaction time 4 hours. M.p. 155°-157°C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS03951957
Source datasetuspto-grants-1976_04
ORD IDord-5e4d95e3d6de4f3ebc58654e503d21ad
Source noteuspto-grants-1976_04