Hydrochloric Acid → HCID 12653318, compound

HRID 1605855Notes

Reaction equation

HRID 1605855 reaction equation
[CH3:1][C:2]([CH3:6])([OH:5])[C:3]#[N:4].[CH2:7]([O:9]CC)[CH3:8].[ClH:12]>C(O)C>[ClH:12].[CH3:1][C:2]([CH3:6])([OH:5])[C:3](=[NH:4])[O:9][CH2:7][CH3:8]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 6406Acetone Cyanohydrin

Product 1

HCID 12653318HCID 12653318, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Four grams of 2-methyllactonitrile is added to 100 ml. of diethyl ether containing 10 ml. of ethanol followed by saturation of the resulting solution with hydrogen chloride gas. The reaction mixture is allowed to stir at room temperature for 18 hrs. and subsequently concentrated to an oil which on slurrying in ether gave 7.2 g. of the desired product.

Workup

  1. concentrationand subsequently concentrated to an oil which on slurrying in ether
  2. customgave 7.2 g

Sources & evidence

ORD record
ord-1e6f0be53f5242349577d3aea6e26607
Source dataset
uspto-grants-1976_04
Patent number
US03951952

Reaction notes

Loading…