HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20355333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1-Phenylpiperazine | HCID 7096 | — |
| Reactant | HCID 20355330 | HCID 20355330 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20355333 | HCID 20355333 | — |
Reaction Steps
A solution of 7-hydroxy-10-(methylthio)-4H-thieno[3,4-b][1,5]benzodiazepine in excess N-phenylpiperazine and glacial acetic acid is heated at 140°-160°C. for 2 days. The solution is poured into water and the product is collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03951981 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-270b8257bd1345f7bdf40307936ab722 |
| Source note | uspto-grants-1976_04 |