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HRID1605930

反应详情

EQUATION

反应方程式

HRID 1605930 的结构方程式

REACTANTS

反应物

2
结构：CCN1CCNCC1
HCID79196

Piperazine, 1-ethyl-

C6H14N2

结构：N#Cc1ccc(-c2ccc(F)cc2)[nH]c1=O
HCID2765203

6-(4-Fluorophenyl)-2-oxo-1,2-dihydropyridine-3-carbonitrile

C12H7FN2O

PRODUCTS

生成物

1
结构：CCN1CCN(c2ccc(-c3ccc(C#N)c(=O)[nH]3)cc2)CC1
HCID21404518

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

From 21.4 g. of 6-(p-fluorophenyl)-1,2-dihydro-2-oxonicotinonitrile and 22.8 g. of N-ethylpiperazine in 200 ml. of dimethyl sulfoxide, there is obtained 6-[p-(4-ethyl-1-piperazinyl)phenyl]-1,2-dihydro-2-oxonicotinonitrile; m.p. 283°-285° (dec.).