HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimetridazole → HCID 327488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimetridazole | HCID 3090 | — |
| Reactant | tert-Butoxy bis(dimethylamino)methane | HCID 79885 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 327488 | HCID 327488 | — |
Reaction Steps
14.1 g. (0.1 mole) of 5-nitro-1,2-dimethylimidazole and 21 g. (0.12 mole) of bis-dimethylamino-tert.-butoxymethane were heated in 90 ml. of dimethylformamide to 130° C. for 15 minutes. After cooling, the red crystals were vacuum-filtered and recrystallized from dimethylformamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03952007 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-ef8209a719824f259c54cc6763cc1889 |
| Source note | uspto-grants-1976_04 |