Sodium Bicarbonate → 5-(3-Methylbutoxy)-8-propyl-1-thiachromone-2-carboxylic acid sodium salt

HRID 1606108Notes

Reaction equation

HRID 1606108 reaction equation
[CH3:1][CH:2]([CH3:23])[CH2:3][CH2:4][O:5][C:6]1[CH:15]=[CH:14][C:13]([CH2:16][CH2:17][CH3:18])=[C:12]2[C:7]=1[C:8](=[O:22])[CH:9]=[C:10]([C:19]([OH:21])=[O:20])[S:11]2.C(=O)(O)[O-].[Na+:28]>O>[Na+:28].[CH3:23][CH:2]([CH3:1])[CH2:3][CH2:4][O:5][C:6]1[CH:15]=[CH:14][C:13]([CH2:16][CH2:17][CH3:18])=[C:12]2[C:7]=1[C:8](=[O:22])[CH:9]=[C:10]([C:19]([O-:21])=[O:20])[S:11]2

Participants

4

Reactant 2

HCID 516892Sodium BicarbonateHCID 215459705-(3-Methylbutoxy)-8-propyl-1-thiachromone-2-carboxylic acid

Product 1

HCID 1317101435-(3-Methylbutoxy)-8-propyl-1-thiachromone-2-carboxylic acid sodium salt

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

5.9 Parts of 5-(3-methylbutoxy)-8-propyl-1-thiachromone-2-carboxylic acid was reacted with 1.83 parts of sodium bicarbonate in 50 parts of water. The resulting yellowish solution was freeze dried to give 5.7 parts of 5-(3-methylbutoxy)-8-propyl-1-thiachromone-2-carboxylic acid sodium salt.

Workup

  1. customdried

Sources & evidence

ORD record
ord-90106e7d26384e7ea163851889f4c65e
Source dataset
uspto-grants-1976_04
Patent number
US03952013

Reaction notes

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