Hydrochloric Acid → HCID 21545995, compound

HRID 1606110Notes

Reaction equation

HRID 1606110 reaction equation
[CH3:1][CH:2]([CH3:14])[CH2:3][CH2:4][O:5][C:6]1[CH:7]=[CH:8][C:9]([CH3:13])=[C:10]([CH:12]=1)[NH2:11].[ClH:15]>CCOCC>[ClH:15].[CH3:1][CH:2]([CH3:14])[CH2:3][CH2:4][O:5][C:6]1[CH:7]=[CH:8][C:9]([CH3:13])=[C:10]([CH:12]=1)[NH2:11]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 21545963HCID 21545963, compound

Product 1

HCID 21545995HCID 21545995, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

A solution of 1 part of 5-(3-methylbutoxy)-2-methylaniline in 50 parts of ether was treated with anhydrous hydrogen chloride gas until no further precipitation occurred. The precipitate was filtered off and dried to leave 1.2 parts of 5-(3-methylbutoxy)-2-methylaniline hydrochloride as a grey powder.

Workup

  1. filtrationThe precipitate was filtered off
  2. customdried

Sources & evidence

ORD record
ord-3c530215d999403a83d05c6507248379
Source dataset
uspto-grants-1976_04
Patent number
US03952013

Reaction notes

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