HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 54512127, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 21545860 | HCID 21545860 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54512127 | HCID 54512127 | — |
Reaction Steps
A suspension of 8.0 g. (0.025 mole) of ethyl 5-(p-chlorobenzoyl)-1-methylpyrrole-2-propionate in 15 ml. ethanol and 30 ml. 1N sodium hydroxide is refluxed for 1 hour. The ethanol is then evaporated and the remaining solution is poured into dilute hydrochloric acid. The resulting white precipitate is filtered off and purified by recrystallization from isopropyl alcohol, 5-(p-chlorobenzoyl)-1-methylpyrrole-2-propionic acid, m.p. 188°-191°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03952012 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-8dbf896725034782bba4f921cef0fafd |
| Source note | uspto-grants-1976_04 |