HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 5-Benzyloxy-2-methylpyridine 1-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 5-(Benzyloxy)-2-methylpyridine | HCID 12397251 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 5-Benzyloxy-2-methylpyridine 1-oxide | HCID 12397252 | — |
Reaction Steps
A solution of 38.1 g. (0.1915 mol) of 5-benzyloxy-2-methylpyridine in 1 l. of chloroform is treated at 25°C. with 42.7 g. of 85% m-chloroperbenzoic acid. Ater one hour the solution is washed with 5% aqueous sodium carbonate, water, dried and evaporated to give 5-benzyloxy-2-methylpyridine-N-oxide, m.p. 87°-89°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03952101 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-4a5d2103d978412ea3f2082c07f9c2ba |
| Source note | uspto-grants-1976_04 |