HRID1606305

反应详情

EQUATION

反应方程式

HRID 1606305 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 38.1 g. (0.1915 mol) of 5-benzyloxy-2-methylpyridine in 1 l. of chloroform is treated at 25°C. with 42.7 g. of 85% m-chloroperbenzoic acid. Ater one hour the solution is washed with 5% aqueous sodium carbonate, water, dried and evaporated to give 5-benzyloxy-2-methylpyridine-N-oxide, m.p. 87°-89°C.

WORKUP

后处理

  1. washAter one hour the solution is washed with 5% aqueous sodium carbonate, water
  2. customdried
  3. customevaporated