HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 21546446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 4-Methoxyphenethyl alcohol | HCID 69705 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Ammonia | HCID 222 | — |
| Product | HCID 21546446 | HCID 21546446 | — |
Reaction Steps
A solution of 40 g of 2-(4-methoxyphenyl)ethanol in 80 ml of ethanol and 800 ml of ammonia reduced with 30.4 g of sodium to yield 27.4 g, bp 87°-89° (0.7 mm), identified by nmr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03952114 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-57ac1f9560484fcfa1efda0b286a556a |
| Source note | uspto-grants-1976_04 |