Sodium Hydroxide → HCID 21542730, compound

Participants

Reaction Steps

10.5 grams of azeloylchloride were placed in a container holding 140 milliliters of tetrachloroethylene and dissolved. To the resulting mixture were added 9.2 grams of N-methyl-N-hexylamine, and 1.6 grams of NaOH dissolved in 200 milliliters of water. The completed mixture was agitated for 10-15 minutes; afterwards the organic layer was separated, washed with a dilute aqueous HCl solution. Following this the organic layer was washed with a 10% aqueous Na2CO3 solution and then washed with water. The washed organic layer was dried by contacting with MgSO4 and then the tetrachloroethylene was removed by application of a vacuum.

Provenance & Evidence